CARATTERIZZAZIONE STRUTTURALE DI MOLECOLE ORGANICHE

The student will acquire the basic knowledge and methodology for analysis of MS, IR, UV-Vis and NMR spectra. As final goal, the students will be able to carry out a complete structural and stereochemical characterization of organic molecules, including the possible use of advanced NMR methods.

Introduction – Mass Spectrometry – Molecular formula and MS fragmentations – IR Spectroscopy – UV-Vis Spectroscopy - Theoretical introduction to NMR spectrometry – Instrumentation and safety rules - ¹H NMR spectra - ¹³C NMR spectra - NMR spectra and molecular structure - NMR in dynamic processes – Advanced experiments and 2D NMR - NMR spectra of heteronuclei.

1. R.M. Silverstein, F.X. Webster e D.J. Kiemle, IDENTIFICAZIONE SPETTROSCOPICA DI COMPOSTI ORGANICI 2a Edizione, Casa Editrice Ambrosiana (Milano)

2. M. Hesse, H. Meier, B. Zeeh, METODI SPETTROSCOPICI IN CHIMICA ORGANICA, 2a Edizione, EdiSES (Napoli)

3. H. Friebolin, BASIC ONE- AND TWO-DIMENSIONAL NMR SPECTROSCOPY 3rd Revised edition, Wiley-VCH (Weinheim)

4. Slides of the lessons, available on STUDIUM